Origin Standard

GB/T 514-2005 Technical conditions for glass liquid thermometers for petroleum product testing

AI-translated method card — human verification pending. This is not an official translation of the standard. Unclear source values remain unverified; check the original standard and product certificate before use.

Card type: Product standard

1. Standard number / full title / replacement relationship / publication and implementation

2. Scope of application and grade classification

3. Technical requirements (index table, item by item: item | index | test method standard number)

3.1 General requirements (Chapter 7)

Item Index Test method standard number
Glass Shall comply with the requirements of relevant professional standards; stress shall minimize the possibility of damage caused by heating or mechanical vibration; the temperature-sensing bulb glass shall undergo appropriate thermal stability treatment; the clarity of the engraved lines shall not be affected by glass dullness or turbidity; the meniscus shall not be distorted by glass defects or impurities not provided in the available source
Temperature-sensing liquid (mercury/mercury-based alloy) Must be pure and dry, free of bubbles and other impurities; mercury shall comply with the No. 1 mercury requirements in GB 913 GB 913
Temperature-sensing liquid (ethanol/organic liquid) Must be pure, free of organic impurities, fibers, and other inclusions visible to the eye, and no bubbles shall precipitate out; a dye that does not adhere to glass, does not easily fade, and does not precipitate shall be used for coloring; the coloring shall be stable and obvious, and shall not leave traces on the inner wall of the capillary not provided in the available source
Evaporation and condensation of temperature-sensing liquid Shall not evaporate or condense under normal pressure within the temperature measurement range not provided in the available source
Filling gas The space above the liquid column in the capillary must be filled with dry, pure inert gas at sufficient pressure not provided in the available source
Capillary Shall be straight, with no unevenness or bending detectable by the eye; the capillary bore cross-section shall be circular or elliptical (the major axis of the ellipse at right angles to the viewing surface), with a uniform inner diameter, and no visible contraction or expansion within the reading range not provided in the available source
Inner and outer surfaces of the capillary Shall not be rough or dirty, and there shall be no bubbles affecting readings within the scale range not provided in the available source
Buffer space There must be a buffer space above the upper-limit engraved line (safety bulb or extended capillary bore), and its volume shall be greater than the volume expanded at the upper-limit temperature 20°C; low-temperature thermometers shall be able to withstand the liquid expansion amount at an ambient temperature of 60°C not provided in the available source
Liquid column movement Must be uniform, without jumping, shall not leave traces on the tube wall, and shall not split into segments not provided in the available source
Straight-stem enamel band A milky white (or colored) enamel band with a width not less than one quarter of the outer circumference of the stem shall be fused along the capillary; no enamel band is allowed above the upper-limit temperature 300°C not provided in the available source
Enclosed-scale inner-core capillary Shall pass through the center of the scale and be perpendicular to the scale plate markings; lateral displacement shall not exceed the range of the shortest engraved line length; the distance from the scale plate shall not be greater than 1 mm; longitudinal relative displacement shall not be greater than one half of the smallest scale division not provided in the available source
Enclosed-scale tying The inner-core capillary shall be tied to the scale plate with copper wire of diameter 0.2 mm to 0.3 mm, with no more than two tying points, and the copper wire shall be corrosion-resistant not provided in the available source
Outer tube The enclosed-scale outer tube shall be cylindrical, gradually contracting at the bottom end of the scale plate, and the outer tube thickness shall not be less than 0.6 mm; the inner and outer surfaces shall have no scratches or other defects affecting strength, and the front shall not be rough, nor have bubbles, nodules, or other blemishes not provided in the available source
Capillary gap dimensions See 7.6.1.1 to 7.6.1.4 and 7.6.2 (when the lowest scale line is ≤100°C, the minimum length between the temperature-sensing bulb and the lowest scale line is 13 mm; when >100°C, 30 mm; the minimum between the intermediate bulb and the scale line below it is 5 mm; between the intermediate bulb and the scale line above it, when ≤100°C, 10 mm, and when >100°C, 30 mm; above the highest scale line, when there is a safety bulb, the minimum is 10 mm, and when there is no safety bulb, 30 mm; the volume of the safety bulb shall not be less than the volume equivalent to 20 mm of normal capillary; the intermediate bulb shall be long and narrow, and its position shall be at least 10 mm below the immersion depth line) not provided in the available source
Scale and engraved lines See 7.7.1 to 7.7.9; the maximum engraved line width shall comply with the provisions of Table 4; the ratio of engraved line length to scale width shall comply with Table 5 not provided in the available source
Immersion depth line For partial-immersion thermometers, a permanent immersion depth line shall be marked on the front at a distance from the temperature-sensing bulb corresponding to the immersion depth ±0.5 mm specified in Table 1 not provided in the available source
Top finish The top of a straight-stem thermometer may be smooth-finished, ring-shaped, or button-shaped, and the outer diameter of the ring or button shall not be greater than the outer diameter of the stem; the top of an enclosed-scale thermometer shall be smooth and spherical not provided in the available source
Metal sleeve Engler viscosity No. 1 and No. 2, closed-cup flash point No. 1 and No. 2, and dropping point No. 1 and No. 2 thermometers shall all have a metal sleeve that can be fixed on the apparatus; the accuracy check of thermometers for Engler viscosity and closed-cup flash point determination shall be carried out with the metal sleeve attached not provided in the available source

3.2 Technical specifications for each thermometer

3.3 Thermometer numbers and names (Table 1)

Number Name Temperature range/°C Immersion depth/mm Scale division/°C Applicable method standard number
GB-1 Closed-cup flash point No. 1 (enclosed-scale) -30 to 170 55 1 GB/T 261
GB-2 Closed-cup flash point No. 2 (enclosed-scale) 100 to 300 55 1 GB/T 261
GB-3 Open-cup flash point No. 1 (enclosed-scale) 0 to 360 45 1 GB/T 267, GB/T 509
GB-4 Open-cup flash point No. 1 0 to 360 45 1 GB/T 267, SH/T 0059, SH/T 0561
GB-5 Open-cup flash point No. 2 -6 to 400 25 2 GB/T 3536
GB-6 Engler viscosity No. 1 (enclosed-scale) 0 to 60 90 0.5 GB/T 266
GB-7 Engler viscosity No. 2 (enclosed-scale) 50 to 110 90 0.5 GB/T 266
GB-8 Asphalt Engler viscosity 19 to 27 90 0.1 SH/T 0099.1
GB-9 Kinematic viscosity No. 1 (enclosed-scale) 98 to 102 Full immersion 0.1 GB/T 265
GB-10 Kinematic viscosity 2 number (internal standard type) 78~82 Full immersion 0.1 GB/T 265
GB-11 Kinematic viscosity 3 number (internal standard type) 48~52 Full immersion 0.1 GB/T 265
GB-12 Kinematic viscosity 4 number (internal standard type) 38~42 Full immersion 0.1 GB/T 265
GB-13 Kinematic viscosity 5 number (internal standard type) 18~22 Full immersion 0.1 GB/T 265、SH/T 0685
GB-14 Kinematic viscosity 6 number (internal standard type) -2~2 Full immersion 0.1 GB/T 265
GB-15 Kinematic viscosity 7 number (internal standard type) -22~-18 Full immersion 0.1 GB/T 265
GB-16 Kinematic viscosity 8 number (internal standard type) -32~-28 Full immersion 0.1 GB/T 265
GB-17 Kinematic viscosity 9 number (internal standard type) -42~-38 Full immersion 0.1 GB/T 265
GB-18 Kinematic viscosity 10 number (internal standard type) -52~-48 Full immersion 0.1 GB/T 265
GB-19 Kinematic viscosity 11 number (internal standard type) -62~-58 Full immersion 0.1 GB/T 265
GB-20 Asphalt viscosity 1 number 58.6~61.4 Full immersion 0.05 SH/T 0557
GB-21 Asphalt viscosity 2 number 133.6~136.4 Full immersion 0.05 SH/T 0557
GB-22 Brookfield viscosity 1 number 45~-35 Full immersion 0.1 GB/T 11145
GB-23 Brookfield viscosity 2 number -35~-25 Full immersion 0.1 GB/T 11145
GB-24 Brookfield viscosity 3 number -25~-15 Full immersion 0.1 GB/T 11145
GB-25 Brookfield viscosity 4 number -15~-5 Full immersion 0.1 GB/T 11145
GB-26 Dropping point 1 number (internal standard type) 0~150 Full immersion 1 SH/T 0115
GB-27 Dropping point 2 number (internal standard type) 100~250 Full immersion 1 SH/T 0115
GB-28 Dropping point 3 number -5~300 76 1 GB/T 4929、SH/T 0089、SH/T 0430
GB-29 Dropping point 4 number -5~400 76 1 GB/T 3498、GB/T 8019、SH/T 0661
GB-30 Freezing point (internal standard type) -30~60 150 1 GB/T 510
GB-31 Crystallization point, freezing point 1 number (internal standard type) -80~60 75 1 SH/T 0179、SH/T 0644
GB-32 Crystallization point, freezing point 2 number (internal standard type) -60~60 75 1 SH/T 0179
GB-33 Paraffin wax congealing point 20~100 Full immersion 0.5 SH/T 0132
GB-34 Melting point 38~82 79 0.1 GB/T 2539
GB-35 Paraffin wax dropping point, melting point 32~127 79 0.2 GB/T 8026、SH/T 0100
GB-36 Cloud point, pour point 1 number -80~20 76 0.5 GB/T 3535、GB/T 6986、SH/T 0030、SH/T 0248
GB-37 Cloud point, pour point 2 number -38~50 108 0.2 GB/T 3535、GB/T 6986、SH/T 0030、SH/T 0603、SH/T 0248
GB-38 Ice point -80~20 Full immersion 0.2 GB/T 2430
GB-39 Coolant freezing point 1 number -37~2 100 0.2 SH/T 0090
GB-40 Coolant freezing point 2 number -54~-15 100 0.2 SH/T 0090
GB-41 Benzene crystallization point 4~6 Full immersion 0.02 GB/T 3145
GB-42 Softening point 30~180 Full immersion 0.5 GB/T 4507、SH/T 0639
GB-43 Brittle fracture point -38~30 Full immersion 0.2 GB/T 4510
GB-44 Distillation 1 number (internal standard type) 0~360 Full immersion 1 GB/T 255
GB-45 Distillation 2 number 0~360 Full immersion 1 GB/T 255
GB-46 Distillation 3 number -2~300 Full immersion 1 GB/T 6536、SH/T 0326
GB-47 Distillation 4 number -2~400 Full immersion 1 GB/T 6536
GB-48 Lubricating oil foaming -20~102 Full immersion 0.2 GB/T 12579、GB/T 1884、SH/T 0068
GB-49 Coolant foaming 20~150 76 0.1 SH/T 0066
GB-50 Liquefied gas volatility -50~5 35 0.1 GB/T 13287
GB-51 Evaporation loss 1 number 95~155 Full immersion 0.5 GB/T 7325
GB-52 Evaporation loss 2 number 155~170 Full immersion 0.1 GB/T 5304、GB/T 11964
GB-53 Rust-preventive oil evaporation 100~115 Full immersion 0.2 SH/T 0035
GB-54 Vapor pressure 1 number 34~42 Full immersion 0.2 GB/T 6602、GB/T 8017
GB-55 Vapor pressure 2 number 40~70 Full immersion 0.1 GB/T 6602
GB-56 Demulsification -1~105 Full immersion 0.1 SH/T 0191
GB-57 Oxidation characteristics 1 number 80~100 76 0.1 GB/T 12581、SH/T 0565
GB-58 Oxidation characteristics 2 number 72~126 100 0.2 GB/T 12581, SH/T 0124, SH/T 0565
GB-59 Oxidation stability 1 number 98~152 100 0.2 GB/T 12580, SH/T 0722
GB-60 Oxidation stability 2 number 95~103 Full immersion 0.1 GB/T 7325, GB/T 8018, SH/T 0060, SH/T 0325, SH/T 0585, SH/T 0702
GB-61 Thermal stability 1 number 165~180 Full immersion 0.5 SH/T 0560
GB-62 Thermal stability 2 number 145~160 Full immersion 0.5 SH/T 0560
GB-63 Thermal stability 3 number 130~145 Full immersion 0.5 SH/T 0560
GB-64 Ageing characteristics 195~205 100 0.1 GB/T 12709, SH/T 0192
GB-65 Density 1 number -5~25 Full immersion 0.1 GB/T 13377
GB-66 Density 2 number 20~45 Full immersion 0.1 GB/T 13377
GB-67 Density 3 number 40~65 Full immersion 0.1 GB/T 13377
GB-68 Density 4 number -1~38 Full immersion 0.1 GB/T 1884
GB-69 Liquefied gas density -15~45 Full immersion 0.2 SH/T 0221
GB-70 Paraffin wax oil content -37~21 76 0.5 GB/T 3554, SH/T 0638
GB-71 Paraffin wax needle penetration 25~55 Full immersion 0.1 GB/T 4985
GB-72 Oil tank thermometer 1 number -34~52 Full immersion 0.5 GB/T 8927
GB-73 Oil tank thermometer 2 number -16~82 Full immersion 0.5 GB/T 8927
GB-74 Oil tank thermometer 3 number 50~240 Full immersion 1 GB/T 8927
GB-75 Aniline point 1 number 38~42 50 0.2 GB/T 262
GB-76 Aniline point 2 number 25~105 50 0.2 GB/T 262
GB-77 Aniline point 3 number 90~170 50 0.2 GB/T 262

Note: Table 1 contains garbled temperature ranges, immersion depths, scale divisions and method references in the source transcription. Verify each affected specification against the original table before selecting or using a thermometer; the transcribed table is not a verified instrument specification.

3.4 Temperature range table (Table 2)

Table 2 lists temperature ranges, immersion depths, and thermometer numbers grouped by scale division values 0.02°C, 0.05°C, 0.1°C, 0.2°C, 0.5°C, 1°C, 2°C (for details see Table 2 in the original text).

4. List of referenced test methods

5. Inspection rules, sampling

6. Marking, packaging, transportation, storage

7. Quick Reference Q&A

Question Key Answer Points
Which version does this standard replace? Replaces GB/T 514—1983; previous versions are GB 514—1965, GB 514—1975, GB/T 514—1983
What does this standard apply to? Specification requirements for liquid-in-glass thermometers used for temperature measurement in petroleum product test methods (Chapter 1)
How many types of thermometers are there by structure? Solid-stem thermometers and enclosed-scale thermometers (Chapter 4)
What are the thermometric liquids? Mercury (quicksilver), ethanol, or mercury-based alloy (Chapter 4)
What is the temperature scale based on? The 1990 International Temperature Scale (ITS-90), graduated in degrees Celsius (Chapter 5)
Thermometer number range? GB-1 to GB-77 (Table 1)
Where are the technical specifications for enclosed-scale thermometers? Table 3 (Figure 2 to Figure 10)
Where are the technical specifications for solid-stem thermometers? Table 4 (Figure 11 to Figure 18)
What shall mercury thermometric liquid comply with? It shall comply with the requirements for No. 1 mercury in GB 913 (7.2.1)
Thickness requirement for the outer tube of enclosed-scale thermometers? Not less than 0.6 mm (7.5.1)
Distance between the inner capillary tube and the scale plate of enclosed-scale thermometers? Shall not be greater than 1 mm (7.4.6)
Diameter of the copper wire tied for enclosed-scale thermometers? 0.2 mm to 0.3 mm, with no more than two tying points (7.4.7)
Safety bulb volume requirement? Not less than the volume equivalent to 20 mm of normal capillary (7.6.1.4)
Position requirement for the intermediate bulb? Shall be at least 10 mm below the immersion depth line (7.6.2)
Tolerance for the immersion depth line marking of partial-immersion thermometers? Immersion depth ±0.5 mm as specified in Table 1 (7.8)
Which thermometers require a metal sheath? Engler viscosity 1, 2; closed-cup flash point 1, 2; dropping point 1, 2 (7.10)
What regulation is verification based on? JJG 50 Verification Regulation for Liquid-in-Glass Thermometers for Petroleum Products (8.2.1)
What is the maximum verification period? Shall not exceed 1 years (8.2.2)
Prerequisite for using thermometers? Shall be used within the valid verification period and accompanied by a verification certificate (8.2.3, 8.2.4)
What does the marking include? Thermometer number, manufacturer's trademark, CMC metrological mark, date of manufacture, thermometer name (9.1)
Storage conditions? Indoors at -30°C to 40°C, with a relative humidity not exceeding 80%, free from corrosive gases, and well ventilated (9.2)
What is Annex A? Informative annex, a list of thermometers used in standard test methods for petroleum products (Table A.1)
What is Annex B? Informative annex, correspondence between thermometers specified in this standard and corresponding foreign thermometers (Table B.1)
What is Annex C? Informative annex, reference correction method for the emergent stem temperature of thermometers (Equations C.1, C.2, C.3, Tables C.1, C.2)
Value of k in the emergent stem correction formula? For mercury and mercury-thallium alloy k, it is 0.000 16; for ethanol 0.001 04; for toluene 0.001 03; for pentane 0.001 45 (Annex C.1)

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