SH/T 0173-1992 Technical specifications for glass capillary viscometers
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Card type: Product standard
1. Standard number / full title / replacement relationship / issuance and implementation
- Standard number: SH/T 0173-92
- Full title: Technical specifications for glass capillary viscometers
- Replacement relationship: replaces ZB E30 014-89
- Approval/implementation: approved by China Petrochemical Corporation 1992-05-20, implemented on 1992-05-20
- First issuance: year 1976 (see additional notes)
- Technical committee: technical jurisdiction by the Research Institute of Petroleum Processing
- Drafting organization: drafted under the responsibility of the Research Institute of Petroleum Processing
- Main drafters: Hou Shulan, Yang Tingting
2. Scope of application and model classification
- Scope of application: This standard specifies the technical specifications for glass capillary viscometers; it applies to glass capillary viscometers used for determining the viscosity of petroleum and petroleum products.
- Classification: Glass capillary viscometers are divided into four models according to shape and use:
- Type BMN-1 (see Figure 1): eleven in total, with capillary inner diameters of 0.4, 0.6, 0.8, 1.0, 1.2, 1.5, 2.0, 2.5, 3.0, 3.5 and 4.0 mm respectively.
- Type BMN-2 (see Figure 2): two in total, with capillary inner diameters of 5.0 and 6.0 mm respectively.
- Type BMN-3 (see Figure 3, Cannon-Fenske opaque viscometer): twelve in total, with capillary inner diameters of 0.31, 0.42, 0.54, 0.63, 0.78, 1.02, 1.26, 1.48, 1.88, 2.20, 3.10 and 4.00 mm respectively.
- Type BMN-4 (see Figure 4): six in total, with capillary inner diameters of 1.0, 1.2, 1.5, 2.0, 2.5 and 3.0 mm respectively.
3. Technical requirements (indicator table, itemized: item | indicator | test method standard number)
| Item | Indicator | Test method standard number |
|---|---|---|
| Specifications, dimensions and shape | Shall conform to the provisions of Figures 1, 2, 3 and 4 (3.1) | not provided in the available source |
| Material | Must be made of instrument glass or high-borosilicate glass; the glass must be smooth, transparent, free from scratches, striae and bubbles; all welded joints shall be smooth; the welded joints at both ends of the capillary must be connected into a smooth flared shape, and unevenness is not allowed (3.2) | not provided in the available source |
| Ring-shaped graduation lines a, b, c, d | Shall be clearly engraved on the plane of the straight tube axis and perpendicular to the axis, and shall not have broken lines, with a width not greater than 0.2 mm (3.3) | not provided in the available source |
| Capillary and side tubes | The capillary must be straight; the two side tubes shall be parallel to each other; no observable irregular phenomena such as bulging and bending are allowed (3.4) | not provided in the available source |
| Wall thickness (except the capillary) | 1~1.5 mm; annealing shall be uniform (3.5) | not provided in the available source |
| Bottom of the expanded portion | The bottoms of the expanded portions 5 of Type BMN-1 and Type BMN-2 viscometers and 2 of the expanded portion of Type BMN-4 shall not bulge upward, and residual liquid is not allowed during use (3.6) | not provided in the available source |
| Positions of graduation lines a, b | For Type BMN-1 and Type BMN-2, a ring line a and b shall be engraved between 2 and 3 of the expanded portion and on the capillary 4, and the graduation line of b shall be located at the lower end of the flared shape 5~8 mm (3.7) | not provided in the available source |
| Inner diameter of the capillary, inner diameter of the tube body and inner diameter of the neck between expanded portions for Type BMN-1, Type BMN-2 and Type BMN-4 | See Table 1 (3.8) | not provided in the available source |
| Inner diameter of capillary 2 of Type BMN-3 and inner diameter of the neck between other capillaries or expanded portions | See Table 2 (3.9) | not provided in the available source |
Table 1 (Type BMN-1, Type BMN-2, Type BMN-4)
| Model | Capillary 4 (or 3) inner diameter D / mm | Tube body 1 inner diameter d and inner diameter of the neck between expanded portions 2 and 3 / mm | Volume of bulbs A, C and J mL (±5%) | Volume of bulb D mL (±5%) |
|---|---|---|---|---|
| Type BMN-1 | 0.4±0.05 | 2.0 (superscript requires confirmation against the source standard (source-text extraction)) | not provided in the available source | not provided in the available source |
| Type BMN-1 | 0.6±0.05 | 2.0 (superscript requires confirmation against the source standard (source-text extraction)) | not provided in the available source | not provided in the available source |
| Type BMN-1 | 0.8±0.05 | 2.0 (superscript requires confirmation against the source standard (source-text extraction)) | not provided in the available source | not provided in the available source |
| Type BMN-1 | 1.0±0.05 | 2.0 (superscript requires confirmation against the source standard (source-text extraction)) | not provided in the available source | not provided in the available source |
| Type BMN-1 | 1.2±0.05 | 2.0 (superscript requires confirmation against the source standard (source-text extraction)) | not provided in the available source | not provided in the available source |
| Type BMN-1 | 1.5±0.1 | 2.0 (superscript requires confirmation against the source standard (source-text extraction)) | not provided in the available source | not provided in the available source |
| Type BMN-1 | 2.0±0.1 | 2.0 (superscript requires confirmation against the source standard (source-text extraction)) | not provided in the available source | not provided in the available source |
| Type BMN-1 | 2.5±0.1 | 2.0 (superscript requires confirmation against the source standard (source-text extraction)) | not provided in the available source | not provided in the available source |
| Type BMN-1 | 3.0±0.1 | 2.0 (superscript requires confirmation against the source standard (source-text extraction)) | not provided in the available source | not provided in the available source |
| Type BMN-1 | 3.5±0.1 | 2.0 (superscript requires confirmation against the source standard (source-text extraction)) | not provided in the available source | not provided in the available source |
| Type BMN-1 | 4.0±0.1 | 2.0 (superscript requires confirmation against the source standard (source-text extraction)) | not provided in the available source | not provided in the available source |
| Type BMN-2 | 5.0±0.1 | 5.5 (superscript requires confirmation against the source standard (source-text extraction)) | not provided in the available source | not provided in the available source |
| Type BMN-2 | 6.0±0.1 | 6.5 (superscript requires confirmation against the source standard (source-text extraction)) | not provided in the available source | not provided in the available source |
| Type BMN-4 | 1.0±0.05 | 2.0 (superscript requires confirmation against the source standard (source-text extraction)) | 2.1 | 11 |
| Type BMN-4 | 1.2±0.05 | 2.0 (superscript requires confirmation against the source standard (source-text extraction)) | 2.1 | 11 |
| Type BMN-4 | 1.5±0.1 | 2.5 (superscript requires confirmation against the source standard (source-text extraction)) | 2.1 | 11 |
| Type BMN-4 | 2.0±0.1 | 3.0 (superscript requires confirmation against the source standard (source-text extraction)) | 2.1 | 11 |
| Type BMN-4 | 2.5±0.1 | 3.5 (superscript requires confirmation against the source standard (source-text extraction)) | 2.1 | 11 |
| Type BMN-4 | 3.0±0.1 | 4.0 (superscript requires confirmation against the source standard (source-text extraction)) | 2.1 | 11 |
Note: In Table 1, the column “Tube body 1 inner diameter d and inner diameter of the neck between expanded portions 2 and 3” for Type BMN-1, Type BMN-2 and Type BMN-4 has confused superscripts in source-text extraction, and the specific tolerances require confirmation against the source standard (source-text extraction). The volumes of bulbs A, C and J of Type BMN-4 are listed in the source as 1.6, 2.1, 2.1, 2.1, 2.1, 2.1 (source-text extraction suspected misalignment), and the volume of bulb D is listed in the source as 11 (duplicate), requiring confirmation against the source standard (source-text extraction).
Table 2 (Type BMN-3)
| Viscometer size number | Kinematic viscosity range (mm²/s)/s | Inner diameter of tube 2 mm (±2%) | Inner diameter of tubes 1, 6, C and d mm (±5%) | Constant mm²/s |
|---|---|---|---|---|
| 25 | 0.4~2 | 0.31 | 3.0 | 0.002 |
| 50 | 0.8~4 | 0.42 | 3.0 | 0.004 |
| 75 | 1.6~8 | 0.54 | 3.0 | 0.008 |
| 100 | 3~15 | 0.63 | 3.2 | 0.015 |
| 150 | 7~35 | 0.78 | 3.2 | 0.035 |
| 200 | 20~100 | 1.02 | 3.2 | 0.1 |
| 300 | 50~200 | 1.26 | not provided in the available source | not provided in the available source |
| 350 | 100~500 | 1.48 | not provided in the available source | not provided in the available source |
| 400 | 240~1200 | 1.88 | not provided in the available source | not provided in the available source |
| 450 | 500~2500 | 2.20 | not provided in the available source | not provided in the available source |
| 500 | 1600~8000 | 3.10 | not provided in the available source | not provided in the available source |
| 600 | 4000~20000 | 4.00 | not provided in the available source | not provided in the available source |
Note: 1) the minimum flow time is all 200s.
4. List of referenced test methods
not provided in the available source (this standard is a technical specification; the main text does not list a bibliography of referenced documents).
5. Inspection rules, sampling
- 4.1 Before glass capillary viscometers are sold for use, they shall be inspected in accordance with the provisions of this technical specification.
- 4.2 Glass capillary viscometers shall meet the requirements of this technical specification and shall be accompanied by a verification certificate at the factory.
- Sampling: not provided in the available source.
6. Marking, packaging, transportation, storage
- Marking (Chapter 5): The following markings shall be indicated on the expanded part or the body of the glass capillary:
- a. Manufacturer's name or trademark;
- b. Capillary inner diameter;
- c. Indicate the instrument number;
- d. Year and month of factory release.
- Packaging (Chapter 6): It shall be carried out according to the general packaging requirements for instruments.
- Transportation, storage: not provided in the available source.
7. Quick reference Q&A
| Question | Key answer points |
|---|---|
| What type of standard is this? | Product standard (technical specification), specifying the technical specifications for glass capillary viscometers. |
| Which old standard does it replace? | Replaces ZB E30 014-89. |
| What is it applicable to? | Glass capillary viscometers for determining the viscosity of petroleum and petroleum products. |
| How many models are there? | Four types: BMN-1, BMN-2, BMN-3, BMN-4. |
| How many pieces and what inner diameter range does the BMN-1 type have? | Eleven pieces, 0.4~4.0 mm. |
| How many pieces and what inner diameter does the BMN-2 type have? | Two pieces, 5.0 and 6.0 mm. |
| How many pieces and what inner diameter range does the BMN-3 type have? | Twelve pieces, 0.31~4.00 mm; Cannon-Fenske opaque viscometer. |
| How many pieces and what inner diameter range does the BMN-4 type have? | Six pieces, 1.0~3.0 mm. |
| Material requirements? | Instrument glass or high borosilicate glass; smooth and transparent, free of scratches, striae and bubbles; smooth at the welded joints, and the welded joints at both ends of the capillary shall be smooth and trumpet-shaped. |
| Requirements for the width of the engraved line? | Not greater than 0.2 mm, clear, perpendicular to the axis, and must not be broken. |
| Wall thickness requirements? | Except for the capillary, 1~1.5 mm, uniformly annealed. |
| Position of the b engraved line? | Located at the lower end of the trumpet shape 5~8 mm. |
| Minimum flow time? | Table 2 Note: all are 200s. |
| What must be attached at the factory? | Verification certificate. |
| Marking content? | Manufacturer's name or trademark, capillary inner diameter, instrument number, year and month of factory release. |
| Packaging requirements? | It shall be carried out according to the general packaging requirements for instruments. |
| When was it first published? | 1976 year. |
| Technical committee and drafting organization? | Technical committee and drafting responsibility of the Research Institute of Petroleum Processing. |
| Main drafters? | Hou Shulan, Yang Tingting. |
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